Titanium deposition and loading with gas

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Doug Coulter
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Titanium deposition and loading with gas

Post by Doug Coulter »

My first try at this is over in "it almost worked" because, well, it almost worked. This try worked.
I used 7" of Ta wires, times three, .020" diameter each, and one Ti wire, .032", and this time, loaded it with a 1.5" piece of 1 mil thick Pd foil, about 1/4" wide, wrapped around the middle of this heater.
Heater that works for Ti and Pd just fine, thanks.
Heater that works for Ti and Pd just fine, thanks.
Using the rig depicted in "it almost worked" otherwise, I then ran a depo that worked.
http://www.youtube.com/watch?v=2cr0yJRVFXg

Kind of boring when it works and you're going slowly. At the temps I was creeping up to, this didn't go real fast - except for the Pd if you watch the mica carefully. Not sure that's the best way, but it's the way it happened this time.


So, after doing most of that, I decided to put that last little bit on with D present in normal fusor pressure or a little higher, figuring that if that surface was wonky, I had the good Pd, then Ti under it. It did flake off the mica, but it turned out I had that mica WAY too hot for its health - and at the distance of the tank walls, it didn't flake off the mica either. Turns out though, that this thing really sucked in the D - about 20 times what it normally takes to bring the tank from e-8 mbar up to 2.5e-2. That's a heck of a lot of gas, but I just kept adding more (foreline shut off) and the pressure just kept dropping again, for quite some time.

http://www.youtube.com/watch?v=_NdsyPyqvPA


I'm letting this sit in 1e-1 mbar of D overnight and then I'll put in a new grid with Th doped W rods this time, for grins. If I ever get it really hot, it'll emit electrons better. I expect the Th will get reduced by hot D and some of it will sputter off. We'll see.
Posting as just me, not as the forum owner. Everything I say is "in my opinion" and YMMV -- which should go for everyone without saying.
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